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WEBFirst, 20 g of PCS sample was placed in a ball miller (XQM4L, Changsha Tianchuang Powder Co., Ltd., China). The ball milling parameters were as follows: The proportion of large, medium, and small balls (about 15, 8, and 3 mm in diameter respectively) was 2:5:3, the ball soil ratio was 30:1, and the rotational speed was 500 r/min.
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